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Test Methods for Metal Powders

Laser Particle Size Analysis
Thaisarco operates a Beckman Coulter LS 13 320 Series Laser Diffraction Particle Size Analyser for measuring particle size distribution. Using the Fraunhofer and Mie theories of light scattering, the LS 13 320 Series offers the highest resolution, reproducibility and accuracy within the particle range of 0.04 micron to 2000 micron.

Sieve Analysis
Thaisarco uses the Octagon 2000 sieve shaker as supplied by Endecotts (UK). The following certified sieves are available.

Micron
(ISO 3310)
20
25
38
40
45
53
63
80
125
150
180
200
250
300
315
355
Mesh (BS 410)
635
510
400
-
350
300
240
200
120
100
85
88
60
52
-
44
No. (ASTM)
-
-
400
-
325
270
230
-
120
100
80
-
60
50
-
45

Apparent Density (AD) & Flow Rate
Thaisarco
uses a Hall Flow meter to determine the flow characteristics and apparent density of free flowing metal powders.

By interchanging the standard Hall Flow meter funnel with the Carney Funnel, the instrument can be adapted to determine the apparent density of non free flowing powders (but not their flow rate).
Determines apparent density as per ISO No. 3923/1.
Determines flow rate as per ISO No. 4490.

Chemical Analysis
Atomic Absorption Spectrometry (AAS)

Atomic Absorption Spectrometry (AAS) is used for minor and trace level chemical analysis.
Determines apparent density as per ISO No. 3923/1.
Determines flow rate as per ISO No. 4490.

We operate a flame system and our latest model is a Perkins Elmer AAnalyst 300. The following is an example of our AAS capability.

Elements
Limit of determination
Ag, Be, Ca, Cd, K, Li, Mg, Na, Zn
< 2 ppm
Co, Cu, Cr, Fe, Ni
2-5 ppm
Ba, Bi, In, Pb
5-20 ppm
Al, As, Sb
10-50 ppm
Sn
50-100 ppm

Optical Emission Spectrometer (OES)
Our laboratory operates simultaneous OES systems carrying out multi-element chemical analysis at trace and minor levels on a range of materials after suitable dissolution procedures.

Our latest model is Spectro Lab-NG. The following is an example of our OES capability.

Elements
Limit of determination
Pb, Bi, Cu, Fe, Ni, Co, Ag, Cd, Al, Au, In
1-5 ppm
Sb, Zn
5-10 ppm
As
10 ppm

ICP Optical Emission Spectrometer (ICP-OES)
Thaisarco uses a sequential ICP system carrying out multi-element chemical analysis at trace and minor levels on a range of materials after suitable dissolution procedures. Current model used is a Perkin Elmer Optima 2100DV. The following is an example of our ICP capability.

Elements
Limit of determination
Li, ,Be, Mg, Ca, Sc, Fe, Sr, Cd, Ba,
<0.1 ppb
Na, Al, K, Ti, V, Cr, Mn, Co, Ni, Cu, Zn, Ge, Y, Zr, Nb, Mo, Ru, Ag, In, La, Hf, Ta, W, Re, Ir, Pt, Au, Pr, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm,
0.1-1 ppb
B, C, Si, P, S, Ga, As, Se, Rb, Sn, Sb, Te, Cs, Os, Tl, Pb, Bi, Ce, Nd, Th, U
1-10 ppb
Cl, Br, I
>10 ppb


THAISARCO is ISO9001/ISO14001 registered company

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